Reaction of 1,2,4-triazole-3-thione with acetylene
β Scribed by G. G. Skvortsov; B. V. Trzhtsinskaya; L. F. Teterina; V. K. Voronov; M. N. Popova
- Book ID
- 112329370
- Publisher
- Springer US
- Year
- 1977
- Tongue
- English
- Weight
- 248 KB
- Volume
- 13
- Category
- Article
- ISSN
- 0009-3122
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π SIMILAR VOLUMES
In the title compound, C 16 H 15 N 3 OS, molecules form inversionrelated dimers via N-HΓ Γ ΓS hydrogen bonds. The structure is further stabilized by intermolecularstacking interactions down the a axis.
## Abstract Irradiation of triazole thiones in thinβfilm reactor furnished the corresponding desulfurized triazoles in good yield. The required triazole thiones were synthesized from the respective acid hydrazide and isothiocyanate. Β© 2003 Wiley Periodicals, Inc. Heteroatom Chem 14:269β272, 2003; P