Photodesulfurization of 2,4-diaryl-1,2, 4-triazole-3-thiones
β Scribed by A. Senthilvelan; V. T. Ramakrishnan
- Publisher
- John Wiley and Sons
- Year
- 2003
- Tongue
- English
- Weight
- 81 KB
- Volume
- 14
- Category
- Article
- ISSN
- 1042-7163
- DOI
- 10.1002/hc.10140
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β¦ Synopsis
Abstract
Irradiation of triazole thiones in thinβfilm reactor furnished the corresponding desulfurized triazoles in good yield. The required triazole thiones were synthesized from the respective acid hydrazide and isothiocyanate. Β© 2003 Wiley Periodicals, Inc. Heteroatom Chem 14:269β272, 2003; Published online in Wiley InterScience (www.interscience.wiley.com). DOI 10.1002/hc.10140
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## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a βFull Textβ option. The original article is trackable v
The title compound (C 15 H 12 N 3 OSCl) crystallizes in the monoclinic space group P2 1 /n with a = 11.211( 3), b = 8.106(2), c = 17.494(4) Γ , Ξ² = 104.49(2)ΒΊ, V = 1539.2(7) Γ 3 , Z = 4, D cal = 1.371 Mg/m 3 at T = 293 K. The structure was solved by direct methods and refined by full-matrix least-squ