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Reaction and Characterization of Thioamide Dianions Derived from N -Benzyl Thioamides

โœ Scribed by Murai, Toshiaki; Aso, Hideo; Tatematsu, Yoshiharu; Itoh, Yoshiaki; Niwa, Hisayuki; Kato, Shinzi

Book ID
125930577
Publisher
American Chemical Society
Year
2003
Tongue
English
Weight
129 KB
Volume
68
Category
Article
ISSN
0022-3263

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Generation of sec-thioamide dianions and
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โœ Y. Tamaru; M. Kagotani; Y. Furukawa; Y. Amino; Z. Yoshida ๐Ÿ“‚ Article ๐Ÿ“… 1981 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 194 KB

The enolates of see-thioamides j3, which are generated by three different methods (scheme II and equation l), are alkylated selectively at the c-carbon to the thiocarbonyl group. The unusual i3 '-lithiation to provide an intermediate $i is observed for N-methyl-a,B-dimetylthioacrylamide and N-methyl