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Rare-Earth Metal Alkyl and Hydride Complexes Supported by a Linked Anilido–cyclopentadienyl Ligand: Synthesis, Structure, and Reactivity

✍ Scribed by Dominique Robert; Peter Voth; Thomas P. Spaniol; Jun Okuda

Publisher: John Wiley and Sons
Year: 2008
Tongue: English
Weight: 329 KB
Volume: 2008
Category: Article
ISSN: 1434-1948
DOI: 10.1002/ejic.200800216

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## Abstract The reactions of anhydrous LnCl~3~ (Ln = Y, Nd, Sm, Lu) with two equiv. of sodium __N__,__N′__‐dicyclohexyl‐__N′′__‐bis(trimethylsilyl)guanidinate Na[(Me~3~Si)~2~NC(NCy)~2~], obtained from Na[N(SiMe~3~)~2~] and the 1,3‐dicyclohexyl‐substituted carbodiimide CyN=C=NCy in THF, yield the mo