Rapid synthesis of unsaturated alcohols under mild conditions by highly selective hydrogenation
β Scribed by Tamura, Masazumi; Tokonami, Kensuke; Nakagawa, Yoshinao; Tomishige, Keiichi
- Book ID
- 120420147
- Publisher
- Royal Society of Chemistry
- Year
- 2013
- Tongue
- English
- Weight
- 1009 KB
- Volume
- 49
- Category
- Article
- ISSN
- 1359-7345
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π SIMILAR VOLUMES
Highly rapid and efficient electrophilic substitution reactions of indoles with various aldehydes and ketones were carried out using I 2 in CH 3 CN to afford the corresponding bis(indolyl)methanes in excellent yields.
A series of monoacylated piperazine derivatives were obtained by the reaction of carboxylic acids with 2-chloro-4,6dimethoxy-1,3,5-triazine in dichloromethane at room temperature. Good to excellent yields, short reaction times and mild reaction conditions are important features of this methodology.