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Rapid determination of the ratios of three aromatic residues in peptides by reversed-phase high-performance liquid chromatography with a high-resolution photodiode-array detector

โœ Scribed by Emmanuel Perrin; Laurent Miclo; Alain Driou; Guy Linden

Publisher
Elsevier Science
Year
1995
Weight
643 KB
Volume
664
Category
Article
ISSN
0378-4347

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Simultaneous determination of the two co
Simultaneous determination of the two components of picrotoxin in serum by reversed-phase high-performance liquid chromatography with application to a pharmacokinetic study in rats
โœ R. Soto-Otero; E. Mendez-Alvarez; G. Sierra-Paredes; J. Galan-Valiente; E. Aguil ๐Ÿ“‚ Article ๐Ÿ“… 1989 ๐Ÿ› Elsevier Science ๐ŸŒ English โš– 404 KB

A reversed-phase HPLC method is reported which allows the quantification of picrotin and picrotoxinin in serum. A linear response was obtained for both drugs in the range 0.2-20 micrograms ml-1. The within-day and between-day precisions were 0.8-3.7% and 1.3-4.9%, respectively. The mean recoveries w