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Raman spectra of liquid cyclopropyl cyanide

✍ Scribed by Jacques Maillols; Vlado Tabacik; Serge Sportouch


Publisher
John Wiley and Sons
Year
1981
Tongue
English
Weight
301 KB
Volume
11
Category
Article
ISSN
0377-0486

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Synthesis of cyclopropyl cyanide-2,2-d2
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## Abstract A convenient method for the synthesis of cyclopropyl cyanide‐2,2‐d~2~ has been elaborated. Reduction of methyl 3‐cyanopropionate with lithium borodeuteride followed by reaction of the resulting alcohol with triphenylphosphine and carbon tetrachloride gave 4‐chlorobutyronitrile‐4,4‐d~2~.

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