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Radiochemical purity of β-sitosterols tritiated by catalytic exchange and by the Wilzbach procedure

✍ Scribed by Harold Werbin; I.L. Chaikoff; Miles R. Imada


Book ID
118842844
Publisher
Elsevier Science
Year
1960
Tongue
English
Weight
473 KB
Volume
89
Category
Article
ISSN
0003-9861

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A practical synthesis of [14-3Hldibenz[a, jlacridine and [7-3Hlditfenz [a,hlacridlne is reported from the parent hydrocarbon by catalytic exchange with tritium gas in the presence of palladium on calcium carbonate. Analogous regiospecific labelling with deuterium was also affected. In addition [14-1