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RACEMIZATION BY THE DICYCLOHEXYLCARBODIIMIDE METHOD OF PEPTIDE SYNTHESIS

โœ Scribed by Anderson, George W.; Callahan, Francis M.


Book ID
120013278
Publisher
American Chemical Society
Year
1958
Tongue
English
Weight
294 KB
Volume
80
Category
Article
ISSN
0002-7863

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A new method has been developed for the rapid determination of D-cysteine contents in synthetic peptides. It is based on the reduction of cystine residues, when present, with tris-alkylphosphines, selective derivatization of the cysteine residues with 4-vinylpyridine, followed by acid hydrolysis of