A method has been developed and evaluated for optimization of the selectivity of series-coupled capillary columns in a twin-oven gas chromatographic system in the shortest possible analysis time. The temperatures of either one or both columns were varied independently (partial optimization) or simul
Quantitative optimization of system variables for chromatographic separations : The column temperature
β Scribed by R.J. Laub; J.H. Purnell
- Publisher
- Elsevier Science
- Year
- 1978
- Tongue
- English
- Weight
- 795 KB
- Volume
- 161
- Category
- Article
- ISSN
- 1873-3778
No coin nor oath required. For personal study only.
β¦ Synopsis
Our previously-reported window diagram optimization technique is here extended to the optimization of analysis temperature. Examples drawn from gasliquid chromatography, gas-liquid chromatography and high-performance liquid chromatography are presented_ The generality of the technique is demonstrated and its potential in analytical areas other than chromatography is pointed out.
JNTRODUCl3ON
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