Quantitative energy dispersive x-ray micro-analysis of thin metal specimens using the STEM
β Scribed by P. Schwaab
- Book ID
- 112188130
- Publisher
- Hindawi Limited
- Year
- 1987
- Tongue
- English
- Weight
- 622 KB
- Volume
- 9
- Category
- Article
- ISSN
- 0161-0457
No coin nor oath required. For personal study only.
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Energy-dispersive x-ray Γuorescence in combination with partial least-squares regression (PLSR) was used to determine nickel, copper and arsenic in aqueous solutions. Di β erent spectrum pre-processing methods (square root and logarithmic transformation and top hat Γltering) were used prior to the PL
When analyzing trace elements in an aqueous solution with a droplet method, the major part of the spectral background originates from the scattering of x-rays by the support film. The background is deliberately low when using an ultra-thin polyimide film (0.15 Β΅m thick) as the sample support film. T