✦ LIBER ✦

Pyridine-2,6-dicarbaldehyde bis(benzylidenehydrazone) monohydrate

✍ Scribed by Cheng, Cui-Xia ;Liu, Hao-Wen ;Luo, Fei-Hua ;Cao, Min-Na ;Hu, Zong-Qiu

Publisher: International Union of Crystallography
Year: 2007
Tongue: English
Weight: 403 KB
Volume: 63
Category: Article
ISSN: 1600-5368
DOI: 10.1107/s1600536807022635

No coin nor oath required. For personal study only.

✦ Synopsis

Mo K radiation = 0.09 mm À1 T = 298 (2) K 0.20 Â 0.10 Â 0.10 mm Data collection Bruker SMART CCD area-detector diffractometer Absorption correction: none 11761 measured reflections 2278 independent reflections 1653 reflections with I > 2(I) R int = 0.077 Refinement R[F 2 > 2(F 2 )] = 0.048 wR(F 2 ) = 0.108 S = 0.98 2278 reflections 274 parameters 1 restraint H atoms treated by a mixture of independent and constrained refinement Á max = 0.14 e A ˚À3 Á min = À0.16 e A ˚À3

📜 SIMILAR VOLUMES

[2,6-Bis(2-pyridylamino)pyridine]dinitra

[2,6-Bis(2-pyridylamino)pyridine]dinitratocadmium monohydrate

✍ Fang, Xiao-Niu ;Li, Xin-Fa ;Zeng, Xi-Rui 📂 Article 📅 2005 🏛 International Union of Crystallography 🌐 English ⚖ 414 KB

Tetrabutylammonium bis[N,N′-bis(4-ch

Tetrabutylammonium bis[N,N′-bis(4-chlorophenyl)pyridine-2,6-dicarboxamide(1–)]cobaltate(III) monohydrate

✍ Qi, Jian Ying ;Yang, Qi Yun ;Zhou, Zhong Yuan ;Chan, Albert S. C. 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 375 KB

Diazidobis(2,2′-bipyridine)zinc(II)

Diazidobis(2,2′-bipyridine)zinc(II) monohydrate

✍ Jian, Fangfang ;Li, Chunlei ;Sun, Pingping ;Xiao, Hailian 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 167 KB

Crystal structure analysis of {bis-2,6-(

Crystal structure analysis of {bis-2,6-(3,5-dimethylprazolyl) pyridine-dicyanato}copper(II)monohydrate

✍ C. Arıcı; D. Ülkü; R. Kurtaran; Ü. Ergun; O. Atakol 📂 Article 📅 2006 🏛 John Wiley and Sons 🌐 English ⚖ 149 KB 👁 2 views

A mononuclear copper(II) complex, [Cu(dmpp)(OCN) 2 (H 2 O)], was synthesized using 2,6-bis (3,5dimethylpyrazolyl) pyridine (dmpp) and cyanate anion (OCN), and characterized by single crystal X-ray diffraction. The coordination around the Cu atom is a distorted square-pyramid involving three N atoms

Diaquabis[2,6-bis(1,2,4-triazol-2-yl)p

Diaquabis[2,6-bis(1,2,4-triazol-2-yl)pyridine-κN4]trinitratolathanum(III) monohydrate

✍ Kwak, Han ;Park, Byeong Kwon ;Kim, Cheal ;Kim, Sung-Jin ;Kim, Youngmee 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 312 KB

2,6-Bis[1-(2,6-dimethylphenylimino)eth

2,6-Bis[1-(2,6-dimethylphenylimino)ethyl]pyridine

✍ Huang, Yuan-Biao ;Ma, Xiu-Ling ;Zheng, Si-Ning ;Chen, Jian-Xin ;Wei, Chun-Xia 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 199 KB

In the molecule of the title compound, C~25~H~27~N~3~, the two 2,6-dimethyl-substituted phenyl rings are connected to the pyridine ring __via__ the C=N imine bonds. Although the compound includes three N atoms, there are no obvious hydrogen-bond or π–π interactions in the crystal structure.