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Pyridine-2-carb­aldehyde thio­semicarbazone 1.75-hydrate

✍ Scribed by Jin, Zhi Min ;Shen, Liang ;He, Lin ;Guo, Hong ;Wang, Hua Tong

Publisher
International Union of Crystallography
Year
2003
Tongue
English
Weight
318 KB
Volume
59
Category
Article
ISSN
1600-5368

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✦ Synopsis

Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.003 A Ê R factor = 0.040 wR factor = 0.095 Data-to-parameter ratio = 15.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the title compound, [Pt(C 14 H 19 N 4 S)Cl], the azepane ring is partially disordered over two sites. The Pt atom coordination adopts a slightly distorted square-planar geometry. The 2acetylpyridine thiosemicarbazone moiety is very close to planar. The azepane ring has a (Àsc, +sc) 3 , +sp confor