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Purification of Fluorous Mitsunobu Reactions by Liquid-Liquid Extraction

✍ Scribed by Dennis P. Curran; Reena Bajpai; Elizabeth Sanger


Publisher
John Wiley and Sons
Year
2006
Tongue
English
Weight
82 KB
Volume
348
Category
Article
ISSN
1615-4150

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Headspace solid-phase microextraction (SPME) and continuous liquid±liquid extraction (LLX) with Freon were used to extract and analyse aroma volatiles in brandy. In general, SPME using a non-polar polydimethylsiloxane coating was more selective for esters and acids than was LLX. LLX using Freon 11 e