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Proton Transfer to CpRuH(CO)(PCy3) Studied by Low-Temperature IR and NMR Spectroscopy

✍ Scribed by Natalia V. Belkova; Alexei V. Ionidis; Lina M. Epstein; Elena S. Shubina; Stephan Gruendemann; Nikolai S. Golubev; Hans-Heinrich Limbach

Publisher
John Wiley and Sons
Year
2001
Tongue
English
Weight
402 KB
Volume
2001
Category
Article
ISSN
1434-1948

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The enthalpy and entropy changes relative to the stepwise reaction of [(triphos)Re(CO) 2 H] with perfluoro-tert-butyl alcohol in CH 2 Cl 2 to give first the hydrogen-bonded adduct [(triphos)Re(CO) 2 H•••HOC(CF 3 ) 3 ] and then the stable non-[a] A. N.