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Protection of a protecting group: Preparation of stable N-silylated t-butyl carbamates

✍ Scribed by Johanne Roby; Normand Voyer

Publisher
Elsevier Science
Year
1997
Tongue
French
Weight
197 KB
Volume
38
Category
Article
ISSN
0040-4039

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✦ Synopsis

The practical preparation of N-silylated carbamates (typified by 1) is reported. These compotmds are synthesized in high yields by treating N-t-Boc.protected primary amines with silyl trillate reagents in dichlofomethane in the presence of triethylamine.

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