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Prostaglandin synthesis. II. A novel resolution of aldehyde and ketone intermediates

✍ Scribed by R. Kelly; V. VanRheenen

Book ID
104246966
Publisher
Elsevier Science
Year
1973
Tongue
French
Weight
195 KB
Volume
14
Category
Article
ISSN
0040-4039

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✦ Synopsis

In a separate communication, we described an efficient synthesis leading to FC&, FGF$, PGEl and PGFlcl (1). This synthesis proceeds via intermediates whose only handles for resolution are aldehyde and ketone functionalities. In order that the efficiency of the synthesis might be

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MoKu radiation, Patterson technique, refined against F2, numerical absorption correction, ~(Mo,,) = 10.1 cm-', H atoms freely refined; the calculations were performed with the programs SHELXTL-Plus, SHELXTL, PLATON-94. Depository number CSD-406923. Space group P i , u = 1015 5(1), b =1166.6(1), c =1