✦ LIBER ✦

Preparative scale organic synthesis using a kitchen microwave oven

✍ Scribed by Chen, Shui-Tein; Chiou, Shyh-Horng; Wang, Kung-Tsung

Book ID: 126927931
Publisher: The Royal Society of Chemistry
Year: 1990
Tongue: English
Weight: 306 KB
Volume: 11
Category: Article
ISSN: 0022-4936
DOI: 10.1039/c39900000807

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

The use of microwave ovens for rapid org

The use of microwave ovens for rapid organic synthesis

✍ Richard Gedye; Frank Smith; Kenneth Westaway; Humera Ali; Lorraine Baldisera; Le 📂 Article 📅 1986 🏛 Elsevier Science 🌐 French ⚖ 244 KB

Four different types of organic reactions have been studied and seven different organic compounds have been prepared, under pressure in a microwave oven. Considerable rate increases have been observed.

Scale-Up of Microwave-Assisted Organic S

Scale-Up of Microwave-Assisted Organic Synthesis

✍ Brett A. Roberts; Christopher R. Strauss 📂 Article 📅 2006 🏛 John Wiley and Sons ⚖ 8 KB 👁 2 views

Preparative scale oxygenations of organi

Preparative scale oxygenations of organic molecules in the solid phase using microwave discharge-generated singlet oxygen

✍ John R. Scheffer; M.Dennis Ouchi 📂 Article 📅 1970 🏛 Elsevier Science 🌐 French ⚖ 225 KB

Applications of Microwave in Organic Syn

Applications of Microwave in Organic Synthesis: An Improved One-step Synthesis of Metallophthalocyanines and a New Modified Microwave Oven for Dry Reactions

✍ Villemin, Didier; Hammadi, Mohamed; Hachemi, Messaoud; Bar, Nathalie 📂 Article 📅 2001 🏛 Molecular Diversity Preservation International 🌐 English ⚖ 101 KB

A Large-Scale Synthesis of Enantiomerica

A Large-Scale Synthesis of Enantiomerically Pure Cetirizine Dihydrochloride Using Preparative Chiral HPLC

✍ Pflum, Derek A.; Wilkinson, H. Scott; Tanoury, Gerald J.; Kessler, Donald W.; Kr 📂 Article 📅 2001 🏛 American Chemical Society 🌐 English ⚖ 68 KB

A Large-Scale Synthesis of Enantiomerica

A Large-Scale Synthesis of Enantiomerically Pure Cetirizine Dihydrochloride Using Preparative Chiral HPLC

✍ Pflum, Derek A.; Wilkinson, H. Scott; Tanoury, Gerald J.; Kessler, Donald W.; Kr 📂 Article 📅 2001 🏛 American Chemical Society 🌐 English ⚖ 68 KB

Enantiomerically pure cetirizine can be prepared by preparative HPLC separation of cetirizine amide. The amide has an r value of 2.76 (USP resolution of 8.54) using a Chiralpak AD column, and 0.5 wt % of the amide (based on packing material) can be injected per run.