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Preparation, reactions, and nuclear magnetic resonance spectra of disubstituted derivatives of the octahydrotriborate(1?) ion, [B3H6XX?]?(X = Cl, X?= Cl, NCS, NCBH3, or NCBH2Cl); molecular structure of [B3H6Cl2]? and partial structure of [B3H6Cl(NCS)]?

✍ Scribed by Arunchaiya, Marisa; Morris, John H.; Andrews, Steven J.; Welch, Dorothy A.; Welch, Alan J.

Book ID
121495788
Publisher
The Royal Society of Chemistry
Year
1984
Tongue
English
Weight
1015 KB
Volume
11
Category
Article
ISSN
1472-7773

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## Abstract The preparation of a family of dinuclear monocyclopentadienyl imidoniobium and ‐tantalum complexes was achieved by two different synthetic routes. The diimido complexes [{M(Cp′)Cl~2~}~2~(μ‐1,__i__‐NC~6~H~4~N)] [Cp′ = η^5^‐C~5~H~4~SiMe~3~, M = Nb, __i__ = 4 (1); Cp′ = η^5^‐C~5~H~4~SiMe~3