Using submerged jet electropolishing, extremely thin (< 10 nm), continuous, thermal oxide "windows" have been prepared on polycrystalline titanium (Ti). The preparation technique is described in detail. It has allowed a systematic investigation of the structure of thermal surface oxide layers on Ti
✦ LIBER ✦
Preparation of thin oxide windows on titanium for TEM analysis and protein adsorption studies
✍ Scribed by Göran Rådegran; Lars Mattsson; Ulf Rolander; Jukka Lausmaa; Bengt Kasemo
- Publisher
- Elsevier Science
- Year
- 1990
- Tongue
- English
- Weight
- 194 KB
- Volume
- 21
- Category
- Article
- ISSN
- 0739-6260
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We present a preparation method of cross-sectional thin foils for transmission electron microscopy (TEM). Samples are 0.1±1 mm thick ceramic oxide ®lms (CeO 2 , CeO 2 ±YBa 2 Cu 3 O 7 and CeO 2 ±ZrO 2 /YO 2 ±YBa 2 Cu 3 O 7 ) epitaxially grown on 30±100 mm highly textured nickel substrates. This metho