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Preparation of the [(DippNP) 2 (P 4 ) 2 ] 2+ -Dication by the Reaction of [DippNPCl] 2 and a Lewis Acid with P 4

✍ Scribed by Holthausen, Michael H.; Weigand, Jan J.

Book ID
126130521
Publisher
American Chemical Society
Year
2009
Tongue
English
Weight
508 KB
Volume
131
Category
Article
ISSN
0002-7863

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The preparation of 2-(4-chlorophenyl)-[2
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## Abstract The preparation of 2‐(4‐chlorophenyl)‐[2‐^14^C]thiazol‐4‐ylacetic acid [I.C.I. 54,450] from potassium [^14^C] cyanide in six stages is described. The overall radioachemical yield of product, at a specific activity of 12.56 ΞΌCi/mg, was 22.2%.