Photoelectrochemical behaviour of the SnO2 thin film prepared by ultrasonic spray pyrolysis was studied as a function of deposition time, annealing time and phosphorus content. The photocurrent increased up to 10 min (1.16 ~tm) with deposition time and then decreased. When the SnO2 thin film was ann
Preparation of spherical TiO2/SnO2powders by ultrasonic spray pyrolysis and its spinodal decomposition
โ Scribed by Jong-Heun Lee; Soon-Ja Park
- Publisher
- Springer US
- Year
- 1993
- Tongue
- English
- Weight
- 500 KB
- Volume
- 4
- Category
- Article
- ISSN
- 0957-4522
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โฆ Synopsis
Spherical TiO2/Sn02 powders were prepared from the TiCI4-SnCI 4 aqueous solution by ultrasonic spray pyrolysis. The particle size, particle-size distribution and morphology of the powders were studied in relation to concentration of source solutions and reaction temperatures. The width of the compositional undulation induced by spinodal decomposition in the sintered bodies increased with increasing starting particle sizes, which resulted from micro-compositional heterogeneity in the form of a solid solution within a TiO2/Sn02 secondary sphere.
๐ SIMILAR VOLUMES
Ultrasonic spray pyrolysis using the salt-assisted decomposition method, a process which adds specific salts into a precursor solution, was used to fabricate nano-sized hydroxyapatite (HAp) particles. The added salts (NaNO 3 ) interrupt agglomerate formation of the primary nanoparticles in the synth