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Preparation of Single Crystals of Chromium Thiospinels by Means of Transport Reactions

✍ Scribed by Priv.-Doz. Dr. H. D. Lutz; Dipl.-Chem. Cs. von Lovász


Publisher
John Wiley and Sons
Year
1968
Tongue
English
Weight
122 KB
Volume
7
Category
Article
ISSN
0044-8249

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Preparation and Characterization by AES
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Niobium diselenide powder, \(\mathrm{NbSe}_{2}\), was prepared by direct synthesis from pure elements. Single crystals were obtained by chemical vapor transport (CVT) using iodine as a gas vector in a threezone thermal profile and analyzed by Auger electron spectroscopy (AES). The bulk composition o