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Preparation of Polymer-bonded Chiral Ligand Exchange Chromatographic Stationary Phase and Resolution of Racemates

✍ Scribed by Ma Gui-Juan; Gong Bo-Lin; Yan Chao


Book ID
108499037
Publisher
Elsevier Science
Year
2008
Tongue
Chinese
Weight
248 KB
Volume
36
Category
Article
ISSN
1872-2040

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The enantiomers of several 9-fluorenyl derivatives have been successfully resolved by HPLC on a chiral stationary phase (CSP) based on a mixed 10-undecenoate/3,5dimethylphenylcarbamate of cellulose bonded to allylsilica gel. Previous attempts at resolution, such as NMR methods, GC and the use of a m