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Preparation of N,N-Dimethylacrylamide by Pyrolysis of N,N-Dimethyl-α-Acetoxypropionamide

✍ Scribed by Ratchford, W. P.; Fisher, C. H.

Book ID
126100782
Publisher
American Chemical Society
Year
1947
Tongue
English
Weight
515 KB
Volume
69
Category
Article
ISSN
0002-7863

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The reaction of arylaldehydes 1 and N,N-dimethylacrylamide in the presence of tributylphosphine afforded N,Ndimethyl-3-aroylpropionamides 2 in moderate yields. The reaction might involve the formation of a-oxo ylide A.