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Preparation of nitrile from primary amide (I)

✍ Scribed by Eisaku Yamato; Shigehiko Sugasawa

Publisher
Elsevier Science
Year
1970
Tongue
French
Weight
107 KB
Volume
11
Category
Article
ISSN
0040-4039

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πŸ“œ SIMILAR VOLUMES

Preparation of nitriles from primary ami
Preparation of nitriles from primary amides under Swern oxidation conditions
✍ Noriyuki Nakajima; Makoto Ubukata πŸ“‚ Article πŸ“… 1997 πŸ› Elsevier Science 🌐 French βš– 218 KB

In order to establish a mild conversion method of primary amides to nitriles, various types of carboxc~nides were treated under Sw ern oxidation conditions, ( COCI)2-DMSO and Et3N, as a dehydrating agent to obtain desired nitriles in 75-96% yields.

An efficient chemoselective synthesis of
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An efficient chemoselective method for the preparation of nitriles from primary amides is described which utilizes methyl (carboxysulfamoyl)triethylammonium hydroxide inner salt (Burgess reagent) as the dehydrating reagent.