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Preparation of New Lithium Organotrihydroaluminates: Crystal Structure of {(C4H8O)2Li(.mu.-H)2AlH[C(SiMe2Ph)3]}2

✍ Scribed by Eaborn, Colin; Gorrell, Ian B.; Hitchcock, Peter B.; Smith, J. David; Tavakkoli, Kayumars


Book ID
126298451
Publisher
American Chemical Society
Year
1994
Tongue
English
Weight
264 KB
Volume
13
Category
Article
ISSN
0276-7333

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Two Diorganopotassates: Crystal Structur
✍ Prof. Colin Eaborn; Dr. Peter B. Hitchcock; Dr. Keith Izod; Dr. J. David Smith πŸ“‚ Article πŸ“… 1996 πŸ› John Wiley and Sons 🌐 English βš– 292 KB πŸ‘ 1 views

3a-BF4 To a wlution of I-BF, (0.46g. 1 mmol) in dichloromethane (5 mL) at ~ 50 c' wiis added palladium tetrakis(tripheny1phosphane) (0.86 g. 0 75 mmolj. After \tirriiig for 1X h a t 40 C. the solvent was removed in vacuo. and the reziduc w a \ washed several times with toluene andether to give 3a-BF