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Preparation of Methanesulfonyl Chloride

โœ Scribed by Noller, C. R.; Hearst, P. J.

Book ID
121186536
Publisher
American Chemical Society
Year
1948
Tongue
English
Weight
144 KB
Volume
70
Category
Article
ISSN
0002-7863

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โœ David A Nugiel; Dean A Wacker; Gregory A Nemeth ๐Ÿ“‚ Article ๐Ÿ“… 1997 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 123 KB

Several commercially available hydmxymethylaryl resins were converted to their correslmqading chloromethyl analogs by simple treatment with methanesuifonyl chloride and Hunig's base in DMF at 25 \*(2 over 3 days. This mild method gave quantitative conversions as deamnined by elemental analysis and 1