Preparation of Heptakis(2,6-di-O-ethyl)-β-cyclodextrin and Its Nuclear Magnetic Resonance Spectroscopic Characterization
✍ Scribed by Fumitoshi Hirayama; Masahiko Kurihara; Yasuhide Horiuchi; Tadanobu Utsuki; Kaneto Uekama; Masaki Yamasaki
- Book ID
- 110379626
- Publisher
- Springer US
- Year
- 1993
- Tongue
- English
- Weight
- 838 KB
- Volume
- 10
- Category
- Article
- ISSN
- 0724-8741
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Regio-and stereo-selective reduction of the double bonds in conjugated ketones with numerous reducing agents under various conditions have been studied'. The reactions usually afford mixtures of products, the compositions of which depend on the reagent, the catalyst, the solvent, the pH of the mediu
## Abstract The ^1^H and ^13^C NMR spectra of heptakis(2,6‐di‐__O__‐pentyl)‐β‐cyclodextrin in deuteriochloroform have been fully and unambiguously assigned. Several methods, including homo‐ and heteronuclear spin decoupling, two‐dimensional homo‐ and hetero‐nuclear correlation NMR spectroscopy, spe