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Preparation of .beta.,.gamma.-unsaturated methyl esters from allylic alcohols

โœ Scribed by Whitesell, James K.; Helbling, Andre M.

Book ID
126333252
Publisher
American Chemical Society
Year
1980
Tongue
English
Weight
594 KB
Volume
45
Category
Article
ISSN
0022-3263

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A series of chiral propargylic alcohols with high enantiomeric excess was prepared by asymmetric dihydroxylation of a,b-unsaturated esters, conversion of the diols to 4-(chloromethyl)-1,3-dioxolane intermediates, and base-induced elimination.