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Preparation of benzyl-α-D1-alcohol by the reduction of benzaldehyde with raney alloys in an alkaline deuterium oxide solution

✍ Scribed by Takehito Tsukinoki; Keiko Ishimoto; Hirohisa Tsuzuki; Shuntaro Mataka; Masashi Tashiro

Publisher
John Wiley and Sons
Year
1993
Tongue
French
Weight
186 KB
Volume
33
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

Benzyl‐α‐d~1~‐alcohol was prepared in high isotopic purity by the reduction of benzaldehyde with Raney Cu‐Al alloy in 10% Na~2~CO~3~‐D~2~O solution using ultrasonic irradiation.

📜 SIMILAR VOLUMES

Preparation of deuteriated benzylamines
Preparation of deuteriated benzylamines and phenethylamine with raney alloys in an alkaline deuterium oxide solution
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## Abstract Benzyl‐α,α‐^2^H~2~‐amine, 2‐^2^H~1~‐Benzyl‐α,α‐^2^H~2~‐amine, 3‐^2^H~1~‐Benzyl‐α,α‐^2^H~2~‐amine, 4‐^2^H~1~‐Benzyl‐α,α‐^2^H~2~‐amine, 2, 5‐^2^H~2~‐Benzyl‐α,α‐^2^H~2~‐amine, and phenethyl‐α,α,β,β‐^2^H~4~‐amine were prepared in high isotopic purities from the corresponding benzonitrile, b

Preparation of deuterated naphthalenes,
Preparation of deuterated naphthalenes, anilines, m-toluidines, and anisoles by reductive dehalogenation of the corresponding halogenated derivatives with raney Cu-Al alloy in an alkaline deuterium oxide solution
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## Abstract Four deuterated naphthalenes, ten deuterated anilines, three deuterated m‐toluidines, and five deuterated anisoles were prepared in high isotopic purities from the corresponding halo‐substituted derivatives by the reductive dehalogenation with Raney Cu‐Al alloy in an alkaline deuterium