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Preparation of a Fluorous Protecting Group and Its Application to the Chemoenzymatic Synthesis of Sialidase Inhibitor.

โœ Scribed by Kiyoshi Ikeda; Hitomi Mori; Masayuki Sato

Publisher
John Wiley and Sons
Year
2006
Weight
29 KB
Volume
37
Category
Article
ISSN
0931-7597

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โœ Peter Wipf; Jonathan T. Reeves ๐Ÿ“‚ Article ๐Ÿ“… 2010 ๐Ÿ› John Wiley and Sons โš– 33 KB

Synthesis and Applications of a Fluorous THP Protective Group. -A variety of alcohols (IX) can be protected with a fluorous labeled THP protecting group using the Cp 2 ZrCl 2 -AgClO 4 reagent system to activate the sulfoxide (VII). The protected alcohols (X) can be easily purified by liquid-liquid