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Preparation of a core–shell type MBHA resin and its application for solid-phase peptide synthesis

✍ Scribed by Jeong-Hyun Choi; Tae-Kyung Lee; Jang-Woong Byun; Yoon-Sik Lee

Publisher
Elsevier Science
Year
2009
Tongue
French
Weight
349 KB
Volume
50
Category
Article
ISSN
0040-4039

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✦ Synopsis

a-Amidoalkylation

Partial hydrolysis Solid-phase peptide synthesis a b s t r a c t MBHA (4-methylbenzhydrylamine) resin has been extensively used as a solid support for the synthesis of peptide amides. Herein, we prepared the core-shell-type MBHA resin by benzotriazole-catalyzed amidoalkylation and partial hydrolysis. The core-shell structure of the MBHA resin was confirmed by two-photon microscopy and its synthetic performance in solid-phase peptide synthesis (SPPS) was evaluated.

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