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Preparation of 4,4′-diaminodiphenylmethane-(2H4) for use as internal standard in the quantification of 4,4′-diaminodiphenylmethane

✍ Scribed by Marco Natangelo; Renzo Bagnati; Roberto Fanelli; Marco Gavinelli; Claudia Ulbricht; Emilio Benfenati


Publisher
John Wiley and Sons
Year
1991
Tongue
French
Weight
170 KB
Volume
29
Category
Article
ISSN
0022-2135

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✦ Synopsis


A simple method has been developed for the synthesis of 4,4'-diarninodiphenylmethane-(2Hq) for analytical purposes in gas chromatography-negative ion chemical ionization mass s ectrometry usin deutero-h drochloric acid in deuterated metkanol. The reaction was aromatic rings was observed after eight days in these conditions, using mass spectrometry (MS) and nuclear magnetic resonance (NMR) spectroscopy.


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