✦ LIBER ✦

Preparation of 3H-labelled apomorphine, N-n-propylnorapomorphine, and O, O-dipivaloylapomorphine

✍ Scribed by William H. Soine; Peter Salgo; Robert V. Smith

Book ID: 102372683
Publisher: John Wiley and Sons
Year: 1979
Tongue: French
Weight: 218 KB
Volume: 16
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2580160412

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✦ Synopsis

Abstract

Apomorphine and N‐n‐propylnorapomorphine were tritiated using trifluoroacetic acid‐ tritiated water mixtures. This provides a route to the synthesis of tritiated O,O‐dipivaloylapomorphine. Deuterium exchange and NMR studies indicate that exchange only involves protons at the C‐8 and C‐9 positions.

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