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Aporphines. 28. Preparation of (-)-N-[3H- and -2H]propylnorapomorphine

✍ Scribed by Filer, Crist N.; Ahern, David; Granchelli, Felix E.; Neumeyer, John L.; Law, Say-Jong


Book ID
126954024
Publisher
American Chemical Society
Year
1980
Tongue
English
Weight
393 KB
Volume
45
Category
Article
ISSN
0022-3263

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Preparation of 3H-labelled apomorphine,
✍ William H. Soine; Peter Salgo; Robert V. Smith πŸ“‚ Article πŸ“… 1979 πŸ› John Wiley and Sons 🌐 French βš– 218 KB

## Abstract Apomorphine and N‐__n__‐propylnorapomorphine were tritiated using trifluoroacetic acid‐ tritiated water mixtures. This provides a route to the synthesis of tritiated O,O‐dipivaloylapomorphine. Deuterium exchange and NMR studies indicate that exchange only involves protons at the C‐8 and