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Preparation of 3,4-Dihydroxy-1-benzeneethanol: A Reinvestigation

✍ Scribed by Baraldi, Pier Giovanni ;Simoni, Daniele ;Manfredini, Stefano ;Menziani, Emilia

Publisher
John Wiley and Sons
Year
1983
Tongue
English
Weight
201 KB
Volume
1983
Category
Article
ISSN
0947-3440

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✦ Synopsis

Abstract

A reinvestigation of the two known methods of preparation of the title compound 1 revealed that one of these leads to a mixture of 1 and 4‐[2‐(acetoxy)ethyl]‐1,2‐benzenediol (5). The other method yields only 2‐methoxy‐4‐(2‐phenylethyl)phenol (6). An unambiguous straightforward preparation of 1 by LiAlH~4~ reduction of 3,4‐dihydroxy‐1‐benzeneacetic acid (8) is described.

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