๐”– Bobbio Scriptorium
โœฆ   LIBER   โœฆ

Preparation of 3, 5-dimethylpyrazole-3, 5-14C and its hypoglycemic metabolite, 5-methylpyrazole-3-carboxylic acid-5-14C

โœ Scribed by Richard C. Thomas


Publisher
John Wiley and Sons
Year
1978
Tongue
French
Weight
272 KB
Volume
15
Category
Article
ISSN
0022-2135

No coin nor oath required. For personal study only.

โœฆ Synopsis


3,5-Dimethylpyrazole-3,5-"T and i t s h oglycemic metabo-1 i t e , 5-methyl pyrazole-3-carboxyl i c acid-5-%.

were each prepared by separate two-step reaction sequences from acetone-2-4C i n 38% and 46% yields, respectively.


๐Ÿ“œ SIMILAR VOLUMES


Synthesis of 3-cyano-4-methyl-5(14C)-met
โœ I. L. Honigberg; N. M. Meltzer; C. D. Blanton Jr. ๐Ÿ“‚ Article ๐Ÿ“… 1979 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 181 KB ๐Ÿ‘ 1 views

A synthesis of 3-cyano-4-methyl-5 ( 14 C)-methyl-2-(5-14C)pyrrolyloxamic acid is described. The compound, having specific activity of 66.7 pCi/mmole, was obtained in 19.68% overall yield from uniformly labelled 14C-l-alanine. 14 14 Key Words: 3-Cyano-4-methyl-5( C)-methyl-2-(5-C)pyrrolyloxamic acid,

Synthesis of 14C-labelled showdomycin, 3
โœ H. Minato; Y. Katsuyama; T. Nagasaki; J. Irisawa; K. Igarashi ๐Ÿ“‚ Article ๐Ÿ“… 1978 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 221 KB ๐Ÿ‘ 1 views

PYRROLINE-2,5-DIONE-5-'4C The C-glycosyl nucleoside antibiotic, showdomycin, was first isolated from the culture filtrate o f Streptomyces shawdoensis by Nishimura f i . l r 2 ) o f our laboratory. O n the basis o f spectroscopic studies, chemical transformations, and X-ray crystallographic examinat

Synthesis of [13C5] and [carbonyl-14C]-5
โœ Peter N. Dorff; Mark E. Powell; Charles S. Elmore ๐Ÿ“‚ Article ๐Ÿ“… 2010 ๐Ÿ› John Wiley and Sons ๐ŸŒ French โš– 88 KB

## Abstract The inventory of labeled compounds and methods for their preparation are constantly growing, but still more building blocks of biologically relevant compounds need to be developed. Furans are frequently encountered in bioactive molecules, and a good synthesis of labeled furan is found i