𝔖 Bobbio Scriptorium
✦   LIBER   ✦

Preparation of 2,3-seco-5α-cholestane-2,3-diol and 4α-methyl-2,3-seco-5α-cholestane-2,3-diol and its reactions with o-nitrophenyl selenocyanate

✍ Scribed by Manuel Arnó; MaBegoña García; JoséR. Pedro; Eliseo Seoane

Book ID
118979166
Publisher
Elsevier Science
Year
1984
Tongue
English
Weight
476 KB
Volume
43
Category
Article
ISSN
0039-128X

No coin nor oath required. For personal study only.

📜 SIMILAR VOLUMES

Synthesis of (25S)-5α-cholestane-3β, 26-
Synthesis of (25S)-5α-cholestane-3β, 26-DIOL[2,4,2′,4′-3H4]
✍ Roberto Bovara; Renato Longhi; Francesco Nicotra; Giuseppe Vecchio 📂 Article 📅 1977 🏛 John Wiley and Sons 🌐 French ⚖ 308 KB

## Abstract (25S)–5α‐cholestane‐3β, 26‐diol [2,4,2′,4′–^3^H~4~] was synthesized by hydrogenation of neotigogenin acetate 2, followed by acetylation to (25S)‐5α‐furostane‐3β, 26‐diol diacetate 5; this was oxidized to (25S)–16–22‐dioxo‐5α‐cholestane‐3β, 26‐diol diacetate 6. Clemmensen reduction of th