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Preparation of 2,3-dinitrilo-1,4-dithia-9,10-anthraquinone labelled with 14C or 35S or 14C+35S

✍ Scribed by J. Šeda; M. Fuad; R. Tykva

Publisher
John Wiley and Sons
Year
1978
Tongue
French
Weight
424 KB
Volume
14
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

A method was developed for the preparation of 2,3‐dinitrilo‐1,4‐dithia‐9, 10‐anthraquinone labelled with ^14^C or ^35^S or ^14^C+^35^S on a milligram scale with the use of the semiconducto‐graphic detection. The exchange of the ^35^S radionuclide in various stages of the preparation was examined in detail. By the present method, the following activities were obtained: 88 Ci of ^14^C/mol or 44 Ci of ^35^S/mol or 1.46 Ci of ^14^C + 75 Ci of ^35^S/mol.

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