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Preparation of 1,3-Oxathiolane-2-thiones by the Reaction of Oxirane and Carbon Disulfide

โœ Scribed by Kihara, Nobuhiro; Nakawaki, Yuichi; Endo, Takeshi

Book ID
121326835
Publisher
American Chemical Society
Year
1995
Tongue
English
Weight
295 KB
Volume
60
Category
Article
ISSN
0022-3263

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## Abstract The SnCl~4~โ€catalyzed reaction of (โˆ’)โ€thiofenchone (=1,3,3โ€trimethylbicyclo[2.2.1]heptaneโ€2โ€thione; **10**) with (__R__)โ€2โ€phenyloxirane ((__R__)โ€**11**) in anhydrous CH~2~Cl~2~ at โˆ’60ยฐ led to two spirocyclic, stereoisomeric 4โ€phenylโ€1,3โ€oxathiolanes **12** and **13** __via__ a regiosel