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Preparation of 1,2,3,4,7,7-Hexachlörobicyclo[2.2.1] hepta-2,5-diene by condensation of Hexachlorocyclopentadiene with acetylene

✍ Scribed by A. F. Plate; G. A. Tarasova

Book ID
112489504
Publisher
Springer
Year
1958
Tongue
English
Weight
181 KB
Volume
6
Category
Article
ISSN
1573-9171

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Crystallographic characterization of a stable 7-phosphanorbornadiene-7-oxide: 2,3-benzo-1,4,5,6,7-pentaphenyl-7-phosphabicyclo[2.2.1] hepta-2,5-diene-7-oxide
✍ Christine Gottardo; Stephen Fratpietro; Alan N. Hughes; Mark Stradiotto 📂 Article 📅 2000 🏛 John Wiley and Sons 🌐 English ⚖ 158 KB 👁 1 views

The stable 7-phosphanorbornadiene derivative, 2,3-benzo-1,4,5,6,7-pentaphenyl-7-phosphabicyclo[2.2.1]hepta-2,5-diene-7-oxide (1) was synthesized in 45% yield via the Diels-Alder reaction of pentaphenylphosphole oxide and benzyne. The reaction occurs specifically to give a single isomer, which was ch