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Preparation of 1-substituted bicyclo[2.2.1]heptanes by anionic cyclization of a 5-hexen-1-yllithium

✍ Scribed by Bailey, William F.; Khanolkar, Atmaram D.

Book ID: 127280209
Publisher: American Chemical Society
Year: 1990
Tongue: English
Weight: 621 KB
Volume: 55
Category: Article
ISSN: 0022-3263
DOI: 10.1021/jo00311a028

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## Abstract 1,2 __exo__‐Diiodo‐norbornane (**4**) was prepared from norcamphor hydrazone by oxidative iodination and subsequent rearrangement of the 2,2‐diiodo‐bicyclo [2.2.1]heptane (**2**). The stable α‐iodohydrazone **11** was obtained from 1‐iodo‐bicyclo[2.2.1]heptan‐2‐one (**10**), which itsel