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Preparation and X-ray crystal structure of [Ni(dpdt)2], a novel nickel 1,2-dithiolene complex (H2dpdt = 6-methylene-1,4-dithiepin-2,3-dithiol)

✍ Scribed by Charlton, A.; Underhill, A.E.; Malik, K.M.A.; Hursthouse, M.B.; Jørgensen, T.; Becher, J.

Book ID
123105953
Publisher
Elsevier Science
Year
1995
Tongue
English
Weight
446 KB
Volume
68
Category
Article
ISSN
0379-6779

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Synthesis and crystal structure of [Bu4N
Synthesis and crystal structure of [Bu4N][Ni(mdt)2], a novel nickel dithiolene complex (H2mdt = 2H-1,3-dithiole-4,5-dithiol)
✍ Yvonne S. J. Veldhuizen; Nora Veldman; Anthony L. Spek; Jaap G. Haasnoot; Jan Re 📂 Article 📅 2010 🏛 Elsevier Science 🌐 English ⚖ 222 KB

## Abstract [Bu~4~N][Ni(mdt)~2~] (H~2~mdt = 2__H__‐1,3‐dithiole‐4,5‐dithiol) has been prepared in a three‐step synthesis from [Bu~4~N]~2~[Zn(dmit)~2~] (H~2~dmit = 2‐thione‐1,3‐dithiole‐4,5‐dithiol). The crystal structure is reported which shows that the Ni(mdt)~2~ anion is distorted significantly f