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Preparation and X-ray analysis of a 1:2 adduct of hexamethylenetetramine and thiourea

✍ Scribed by Mak, T. C. W. ;Lau, O. W. ;Ladd, M. F. C. ;Povey, D. C.


Book ID
114525047
Publisher
International Union of Crystallography
Year
1978
Weight
489 KB
Volume
34
Category
Article
ISSN
0567-7408

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A sterically protected diphosphinidenecyclobutene with the 2,4,6-tri-tertbutylphenyl group was allowed to react with tert-butyllithium and iodine, successively, to give 2,2',3,3'-tetraphosphinidene-l,l'-bicyclobutyl derivative, and the structure was confirmed by X-ray analysis, showing unusual short