## NOTES procedure. Thin-layer chromatography allow s a rapid screening of many solutions for evidence of degradation of the preservative materials. The reader should refer to information published elsewhere 1 for a further discussion regarding the complexity of detecting the presence of degradati
✦ LIBER ✦
Preparation and properties of polyamide-sulfonamides
✍ Scribed by Imai, Yoshio ;Okunoyama, Hikaru
- Book ID
- 104536517
- Publisher
- Wiley (John Wiley & Sons)
- Year
- 1972
- Tongue
- English
- Weight
- 352 KB
- Volume
- 10
- Category
- Article
- ISSN
- 0449-296X
No coin nor oath required. For personal study only.
✦ Synopsis
Abstract
A series of polyamide‐sulfonamides was synthesized by the interfacial polycondensation of m‐ and p‐chlorosulfonylbenzoyl chlorides with aliphatic and aromatic diamines at room temperature. Most of the polymers obtained were high molecular weight, film‐forming materials. They were all amorphous and were soluble in a wide range of acidic and basic solvents. Both aliphatic and wholly aromatic polyamide‐sulfonamides showed initial breakdown in the range of 320–360°C under thermogravimetric analysis in a nitrogen atmosphere.
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