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Preparation and polymerization of 2-phenyl-4-methylene-1,3-dioxolane

✍ Scribed by Cai-Yuan Pan; Zhen Wu; W. J. Bailey

Publisher
Wiley (John Wiley & Sons)
Year
1987
Tongue
English
Weight
216 KB
Volume
25
Category
Article
ISSN
0887-6258

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πŸ“œ SIMILAR VOLUMES

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Abstraet--2-(2',4'-Dichlorophenyl)-4-methylene-l,3-dioxolane was synthesized and polymerized by radical (AIBN and photochemically) and cationic (I 2, BF 3 . OEt2) routes. A polymerization mechanism is proposed based on the analysis of the resulting polymers.

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Photoinitiated polymerization of 4-methylene-2-phenyl-1,3-dioxolane ( 1) was carried out using either tris(4-methylphenyl)sulfonium hexafluoroantimonate or 4-decyloxyphenyl phenyliodonium hexafluoroantimonate as initiators. 1 H-NMR analyses confirmed exclusive ring-opening while DSC and SEC were use