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Preparation and Crystal Structure of the Sodium Iodide Complex of 5,11,17,23-tetra(tert-butyl)-25,27-di(ethoxymethoxy)-26,28-(diethylacetamido) Calix[4]arene in the Cone Conformation

✍ Scribed by L. Baklouti; R. Abidi; P. Thuery; M. Nierlich; Z. Asfari; J. Vicens


Book ID
110316153
Publisher
Springer Netherlands
Year
2001
Tongue
English
Weight
70 KB
Volume
40
Category
Article
ISSN
0923-0750

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26,28-Diall­yloxy-5,11,17,23-tetra-tert-
✍ Dordea, Crenguta ;Böhmer, Volker ;Bolte, Michael 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 262 KB

The title compound, C 54 H 66 N 2 O 4 , crystallizes with two molecules in the asymmetric unit. Both adopt the typical partial cone conformation which was also found for 26,28-diallyloxy-5,17-di-tert-butyl-25,27-bis(cyanomethoxy)-11,23-dinitrocalix[4]arene [Danila, Bo ¨hmer & Bolte (2005). Org. Biom