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The crystal structure of the syn-proximal-5,11,17,23-tetra-tert-butyl-25,26-bis[(2-pyridylmethyl)oxy]-27,28-dihydroxy-calix[4]arene ethanol 1 : 1 Inclusion Complex

✍ Scribed by George Ferguson; John F. Gallagher; Sebastiano Pappalardo


Publisher
Springer Netherlands
Year
1992
Tongue
English
Weight
390 KB
Volume
14
Category
Article
ISSN
0923-0750

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26,28-Diall­yloxy-5,11,17,23-tetra-tert-
✍ Dordea, Crenguta ;Böhmer, Volker ;Bolte, Michael 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 262 KB

The title compound, C 54 H 66 N 2 O 4 , crystallizes with two molecules in the asymmetric unit. Both adopt the typical partial cone conformation which was also found for 26,28-diallyloxy-5,17-di-tert-butyl-25,27-bis(cyanomethoxy)-11,23-dinitrocalix[4]arene [Danila, Bo ¨hmer & Bolte (2005). Org. Biom