We report the synthesis and structural characterization of a new oxoanion halide, NaCa 2 GeO 4 F. Crystal data: FW β«Ψβ¬ 235.74, Pnma (No. 62), orthorhombic, a β«Ψβ¬ 5.362(2), b β«Ψβ¬ 7.328(3), c β«Ψβ¬ 12.681(4) A > , V β«Ψβ¬ 498.3(3) A > 3 , Z β«Ψβ¬ 4, R(F) β«Ψβ¬ 0.044, R w (F) β«Ψβ¬ 0.046 for 404 averaged re6ecti
β¦ LIBER β¦
Preparation and Crystal Structure of a New Praseodymium Manganese Germanate: PrMnOGeO4
β Scribed by C. Gueho; D. Giaquinta; P. Palvadeau; J. Rouxel
- Publisher
- Elsevier Science
- Year
- 1995
- Tongue
- English
- Weight
- 251 KB
- Volume
- 120
- Category
- Article
- ISSN
- 0022-4596
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Single crystals of a new reduced calcium niobium oxide, CaNb 2 O 4 , were prepared in an evacuated quartz tube at 11003C. The calcium niobium oxide crystallizes in the orthorhombic space group Pbcm with a β«Ψβ¬ 5.054(1), b β«Ψβ¬ 11.904(1), and c β«Ψβ¬ 5.839(1) A s , Z β«Ψβ¬ 4, and the 5nal R factors are R β«